ASTM E1097-12 (2017) rus PDF

Full title and description

Standard Guide for Determination of Various Elements by Direct Current Plasma Atomic Emission Spectrometry — ASTM E1097-12 (reapproved 2017). This publication provides guidance on using Direct Current Plasma Atomic Emission Spectrometry (DCP‑AES/DCP‑AES) for the determination of elemental concentrations in solution. A Russian-language PDF translation is commercially available.

Abstract

This guide describes recommended procedures for preparing and calibrating a direct current plasma atomic emission spectrometer, assessing instrument performance, diagnosing and correcting interferences, measuring test solutions, and calculating results. It includes instrument drift correction methods and practical guidance rather than prescriptive instrument settings, acknowledging differences between instrument models.

General information

• Status: Withdrawn (catalog records indicate withdrawal effective April 1, 2025).
• Publication date: Designation E1097-12 (reapproved/published 2017). Original revision dated 2012 (E1097-12).
• Publisher: ASTM International.
• ICS / categories: Analytical chemistry for metals, ores and related materials; ICS code noted in records as 71.040.50 (physicochemical methods of analysis).
• Edition / version: E1097-12 (2017) — edition indicated as the 2012 revision with 2017 reapproval notation.
• Number of pages: 8 pages (guide length as listed in standard catalogs).

Scope

This guide covers procedures for using a Direct Current Plasma atomic emission spectrometer to determine concentrations of elements in solution. It gives recommendations for instrument preparation and calibration, performance checks, interference diagnosis and correction, measurement procedures, and calculation of results, but does not specify every operating condition or detailed hardware/software configurations — users must follow instrument manufacturer instructions and verify suitability for their specific instruments and applications.

Key topics and requirements

• Instrument setup and recommended practices for DCP‑AES operation (torch/electrode considerations, sample introduction, spray chamber basics).
• Calibration procedures and standard preparations for quantitative analysis.
• Performance verification and checks (stability, sensitivity, linear dynamic range).
• Identification and correction of spectral, physical and chemical interferences.
• Procedures for measuring test solutions and applying drift-correction methods.
• Safety and laboratory practice notes relevant to DCP operation (general precautionary guidance rather than exhaustive safety requirements).

Typical use and users

Analytical laboratories performing elemental analysis of metals, ores, environmental, and process samples; quality control and R&D laboratories in metals and materials industries; academic research groups using DCP‑AES; instrument manufacturers and service engineers referencing good-practice guidance for method development and troubleshooting.

Related standards

Relevant and related ASTM documents include standards and practices describing DCP instrumentation and specific DCP/ICP test methods (for example, ASTM E1832 for describing and specifying DCP atomic emission spectrometers and ASTM E2371 series for performance-based test methods combining DCP and ICP techniques). Users should consult current ASTM listings for the latest normative and informative references.

Keywords

Direct Current Plasma, DCP‑AES, atomic emission spectrometry, elemental analysis, instrument calibration, interference correction, drift correction, ASTM E1097, analytical chemistry, metals analysis, Russian translation.

FAQ

Q: What is this standard?

A: ASTM E1097-12 (reapproved 2017) is a guide providing recommended procedures and good-practice information for performing elemental determinations by Direct Current Plasma Atomic Emission Spectrometry (DCP‑AES).

Q: What does it cover?

A: It covers instrument preparation, calibration, performance checks, interference diagnosis and correction, measurement procedures, and result calculation methods for DCP‑AES; it is guidance-focused and does not mandate specific instrument settings.

Q: Who typically uses it?

A: Analytical and quality control laboratories (industry and academia) that perform multi-element analysis using DCP‑AES, as well as instrument vendors and service engineers.

Q: Is it current or superseded?

A: Catalog records and standards sellers list E1097-12(2017) as withdrawn (withdrawal effective date shown in vendor records as April 1, 2025). For authoritative current status and any successor documents, consult ASTM International directly.

Q: Is it part of a series?

A: E1097 is part of the ASTM E01 committee area (Analytical Chemistry for Metals, Ores, and Related Materials) and is related to other DCP/ICP standards and practices (for example E1832 and standards in the E2xxx series covering spectrometric methods).

Q: What are the key keywords?

A: DCP, DCP‑AES, direct current plasma, atomic emission spectrometry, elemental analysis, calibration, interference correction, drift correction, ASTM E1097.